Doctoral Candidate (DC2): Characterization of solid-liquid and solid-solid electrochemical interfaces operando at the nanoscale (f/m/d)

Instruct-ERIC; Saarbrücken; Vor Ort; EUR 42.000 - 60.000; Vollzeit

Zusammenfassung

Saarland University in Saarbrücken invites applications for a Doctoral Candidate (DC2) to characterize solid-liquid and solid-solid electrochemical interfaces operando at the nanoscale. The project focuses on Na-ion and Zn-based systems, with advanced STEM and spectroscopy techniques.

The successful candidate will design microbattery setups, conduct operando measurements, and compare results with ex-situ analyses, contributing to a multi-disciplinary team in a cutting-edge research environment.

Qualifikationen

• Excellent communication and writing skills in English.
• Strong knowledge of electrochemistry and materials science.
• Experience with experimental electrochemistry and material characterization is advantageous.

Aufgaben

• Design and test microbattery setups based on MEMS technology.
• Perform operando STEM analyses of S-L and S-S interfaces.
• Collaborate with international teams and compare ex-situ TEM findings.

Kenntnisse

Communication

English proficiency

Electrochemistry

Characterization

Ausbildung

Master's degree in Materials Science / Electrochemistry / Chemistry / Applied Physics

Tools

Electron microscopy

Spectroscopy

STEM methods

MEMS fabrication

Jobbeschreibung

Jobs in Structural Biology and Related Fields

Doctoral Candidate (DC2): Characterization of solid-liquid and solid-solid electrochemical interfaces operando at the nanoscale (f/m/d)

The climate targets set by the EU with the goal of climate neutrality by 2050 require a transformation of all sectors of the economy towards the use of renewables-based electricity, calling for joined forces between EU countries in order to achieve a more resilient energy system. In the e-ChemIn we are united by the idea of applying a new paradigm in designing energy devices, which shifts the current approach of creating individual materials towards engineering electrochemically ACTIVE MATERIALS INTERFACES. Working together we will: 1) design multiple sets of electrochemical interfaces using renewable, abundant, and circular materials and optimize them for new generations of energy conversion and storage devices. Created lab-scale prototypes which outperform characteristics of current benchmarks and will be ready for further developments at high TRLs (5-9); 2) develop multimodal approaches for the characterization of interfaces operando at the nanoscale, providing unprecedented insights into interfaces in action and making the characterization of active interfaces accessible to the broader scientific community; 3) successfully establish processes for the recovery of critical raw materials from end-of-life devices and apply them at the industrial scale.

The aim of the project is to reveal the nanoscale details of the ionic transport at electrode-electrolyte interfaces in operando focusing on the specific role of composite materials in improving sodium ion batteries (SIBs) and zinc ion batteries (ZIBs) performances. The Doctoral Candidate (DC) will design and test microbattery closed-cell setups based on MEMS chip technology and perform operando characterizations of solid-solid (S-S) and solid-liquid (S-L) interfaces using probe corrected scanning transmission electron microscope (STEM) and related spectroscopy techniques. Processes at Na-ion carbonaceous anode and their composites for SIBs will be compared. Zn composite cathodes for ZIBs will be tested. Tight cooperation with DC1 and DC4, assisting with nanoscale characterisation of carbonaceous, composite covalent anode materials in SIBs, and multifunctional ion-conductive polymers in rechargeable aqueous ZIBs, is expected. Operando experiments will be compared with ex-situ TEM analysis of materials from coin cells at different states of charge to ensure comparability of the results. Chemical composition, electronic structure at S-L, S-S and S-S-L interfaces will be probed by EELS.

Expected results

(1) Successful assembly and nanoscale study of the S-L, S-S, S-S-L interfaces in microbattery devices.

(2) Unveiling interface-performances relationships (e.g., composition-porosity-structure with SEI formation for SIBs, ZIBs used within the project).

The selected candidate will be required to enroll in a PhD program at Saarland University.

Supervisors - Benefits - Qualifications

Co-supervisors from secondments:

The Doctoral Candidate will stay 4 months at VSB Technical University of Ostrava (Prof. M. Pumera), Czech Republic and 3 months at Stockholm University (Prof. Jiayin Yuan), Sweden.

Applicants must not already hold a doctoral degree at the date of recruitment and not have resided or carried out their main activity (work, studies, etc.) in Germany for more than 12 months in the 36 months immediately before the recruitment date.

Eligibility will be verified at the time of recruitment.

Skills / Experience

• Excellent communication and writing skills, thorough command of the English language
• Good knowledge of electrochemistry, materials science
• Skills in experimental electrochemistry and electrochemical technologies
• Experience with material characterization using electron microscopy and/or spectroscopy techniques and corresponding data interpretation will be an advantage
• Ability to work as a member of an international, multi-disciplinary team
• German language knowledge is very beneficial.

Master’s degree or equivalent in Materials Science, Electrochemistry, Chemistry, Applied Physics or closely related disciplines.

The deadline for applications is 20 September 2026.

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